Реакция #50870

Уравнение реакции

3-bromothiophenol

potassium carbonate

iodomethane

→

title compound

3-(methylthio)phenylbromide

Растворители

acetone

Условия реакции

Обработка

1. 1
   ТемператураThe heterogenous mixture was refluxed for 4 hrs
2. 2
   Фильтрацияfiltered
3. 3
   Концентрированиеconcentrated under reduced pressure
4. 4
   workup.ADDITIONEther (200 mL) was added
5. 5
   Фильтрацияthe mixture was filtered again
6. 6
   Другоеfinally evaporated to dryness

Методика

To a solution of 3-bromothiophenol (10 g) in acetone (250 mL) was added potassium carbonate (14.6 g) and iodomethane (4.28 mL). The heterogenous mixture was refluxed for 4 hrs., cooled to room temperature, filtered, and concentrated under reduced pressure. Ether (200 mL) was added, and the mixture was filtered again and finally evaporated to dryness to yield the title compound.

Источник