Реакция #4727

ord-e67f7b9458324899aa2bf340325e6943

Уравнение реакции

O=C(NNC(=S)NCCCOc1cccc(CN2CCCCC2)c1)NC1CCCCC1
N-cyclohexyl-2-[[3-[3-(1-piperidinylmethyl)phenoxy]propyl]aminothioxomethyl]-hydrazine carboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride
→
c1cc(CN2CCCCC2)cc(OCCCNc2nnc(NC3CCCCC3)s2)c1
N-Cyclohexyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]1,3,4-thiadiazole-2,5-diamine

Реактанты

O=C(NNC(=S)NCCCOc1cccc(CN2CCCCC2)c1)NC1CCCCC1
N-cyclohexyl-2-[[3-[3-(1-piperidinylmethyl)phenoxy]propyl]aminothioxomethyl]-hydrazine carboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Методика

The compound is prepared by a method analogous to that of Example 40 from N-cyclohexyl-2-[[3-[3-(1-piperidinylmethyl)phenoxy]propyl]aminothioxomethyl]-hydrazine carboxamide and phosphorus oxychloride. The analytical values are summarized in Table III.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US04727081uspto-grants-1988_02