Реакция #470367

Уравнение реакции

Methoxymethylpyrrolidine

dimethyl carbonate

→

desired product

Выход 60.0%

N-Methoxymethyl-N-Methylpyrrolidinium Methyl carbonate

Выход 60.0%

Условия реакции

Обработка

1. 1
   Другоеreacted at 120° C. for 24 hours
2. 2
   ФильтрацияThe resulting solids were filtered off
3. 3
   Промывкаwashed with dimethyl carbonate
4. 4
   ДругоеThe solids were dried in a vacuum

Методика

Methoxymethylpyrrolidine (10.00 g) and 117.39 g of dimethyl carbonate were placed into an autoclave and reacted at 120° C. for 24 hours. The resulting solids were filtered off and washed with dimethyl carbonate. The solids were dried in a vacuum, giving 10.70 g of the desired product.

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