Реакция #452418

Уравнение реакции

levulinic acid

cesium hydroxide

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CESIUM LEVULINATE

Растворители

water

Условия реакции

Обработка

1. 1
   Другоеto obtain complete solution
2. 2
   ФильтрацияThe solution is filtered through No
3. 3
   Фильтрация40 filter paper
4. 4
   Другоеto remove dust, etc. The solution
5. 5
   Другоеis then evaporated on a hot plate to 200 g
6. 6
   Другое, which gives
7. 7
   Концентрированиеa 2 molar concentration, and it

Методика

46.9 gr. of 99% pure levulinic acid is sluurried in 100 cc. distilled water. 97.3 g. of a 4.22 molar, pure cesium hydroxide solution is added and the temperature is raised to 65° C. to obtain complete solution. The solution is filtered through No. 40 filter paper to remove dust, etc. The solution is then evaporated on a hot plate to 200 g., which gives a 2 molar concentration, and it is then bottled.

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