Реакция #443403

ord-5eb6cc29799f4320bb7fc3e47e0a4563

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    workup.ADDITIONwere mixed
  2. 2
    Другоеpolymerized in a bulk state at 60° C. for 24 hours

Методика

According to the ratio for charging as described in Table 2, oxetane and delta-valerolactone (referred to as VL in Table and Figure) were mixed, and polymerized in a bulk state at 60° C. for 24 hours using 0.2% by mol of a triethylaluminum-water (1/0.75) based complex as an initiator based on the total amount of the monomers.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US05834567uspto-grants-1998_11