Реакция #442211

Уравнение реакции

hydrazodicarbonamide

stearyl amine

→

4-stearyl-1,2,4-triazolidine-3,5-dione

Растворители

N-methyl pyrrolidone

Условия реакции

Обработка

1. 1
   ДругоеA deposit precipitates
2. 2
   Температураon cooling
3. 3
   Другоеis isolated by filtration under suction
4. 4
   Промывкаwashed with water

Методика

360 g of hydrazodicarbonamide, 807 g of stearyl amine and 1 ml of tin(II)dioctoate are stirred in 1 liter of N-methyl pyrrolidone for 4 hours at 175° C. and for 6 hours at 200° C. A deposit precipitates on cooling and is isolated by filtration under suction and washed with water, giving 955 g (90% of the theoretical) of 4-stearyl-1,2,4-triazolidine-3,5-dione in the form of colourless crystals melting at 118° to 120° C.

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