Реакция #42063

ord-6e517765710c4ce2aff2f2aa059c94ef

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    Промывкаthat the resulting crude crystals were washed with ethyl acetate

Методика

This compound was prepared in the same manner as in Example 1, except that 4-methyl-3-[4-(5-pyrimidinyl)pyridin-2-ylamino]aniline (Reference Example 22) and 4-(4-ethylpiperazin-1-ylmethyl)-3-trifluoromethylbenzoyl chloride dihydrochloride (Reference Example 5) were used, and that the resulting crude crystals were washed with ethyl acetate.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US07728131B2uspto-grants-2010_06