Реакция #417904
ord-9eb251ab9d2f4dd397596f5f2a9d6088
Уравнение реакции
Desmorapid
n-hexyl isocyanate
isocyanate
→
Isopropyl hexylcarbamate
Реагенты
Нет
Растворители
Условия реакции
Температура
60°CELSIUS
Подробные условия
See reaction.notes.procedure_details.
Обработка
- 1ТемператураThereafter, cooling
- 2Другоеthe product was obtained as a clear liquid
Методика
In a 250 ml round-bottomed flask, 0.02 g of Desmorapid Z, 34.0 g of n-hexyl isocyanate were initially introduced and heated to 60° C. Thereafter, 16.0 g of isopropanol were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, cooling was effected and the product was obtained as a clear liquid.