Реакция #415373

ord-57698e2142ad479dbedb8a5800140627

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    workup.ADDITIONare added in 28 seconds

Методика

To 50 l of an 0.07 M solution of bisodium phosphate, continually stirred by means of a vibrator, 50 l of an 0.07 M solution of calcium chloride are added in 28 seconds; the pH of the mixture is adjusted to 7.1 with a solution of normal sodium hydroxide, following the addition of the CaCl2. The 100 l of calcium phosphate gel thus obtained are left to stand until decantation of 85 l of liquid. The clear supernatant liquid is separated by siphoning and replaced by 85 l of aqueous solution of NaCl, 4 g/l.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US04016252uspto-grants-1977_04