Реакция #3832

Уравнение реакции

2,2'-dithiobisbenzoyl chloride

cyclopropylamine

triethylamine

dichloromethane

dichloromethane

→

title compound

2,2'-Dithiobis(N-cyclopropylbenzamide)

Условия реакции

Обработка

1. 1
   ДругоеA solid formed immediately
2. 2
   Фильтрацияfiltered
3. 3
   ДругоеThe solid was dried

Методика

A solution of 2,2'-dithiobisbenzoyl chloride (1.0 g, 3.0 mmol) in 20 mL of dichloromethane was added dropwise to a solution of cyclopropylamine (0.52 mL, 7.5 mmol) and triethylamine (1.2 mL, 9.0 mmol) in 20 mL of dichloromethane. A solid formed immediately, the mixture was stirred for 3 hours and then filtered. The solid was dried to yield 0.65 g of the title compound, mp 257°-259° C.;

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