Реакция #367490

Уравнение реакции

2-(4-methylphenyl)ethanamine

3-trifluoromethylphenylglyoxal

phenylglyoxal

→

title compound

N-(2-(4-Methylphenyl)ethyl)-2-hydroxy-2-phenylethanamine

Условия реакции

Обработка

1. 1
   ДругоеThe title compound was prepared in the manner
2. 2
   ДругоеThe chromatographed material was recrystallised from hexane

Методика

The title compound was prepared in the manner described in Example 9, replacing 2-(4-methylphenyl)-1,1-dimethylethanamine by 2-(4-methylphenyl)ethanamine and 3-trifluoromethylphenylglyoxal by phenylglyoxal. The chromatographed material was recrystallised from hexane to give the title compound, mp 95°-97°.

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