Реакция #354447

Уравнение реакции

hydrogen chloride

stearyl alcohol

methyl cyano acetate

→

stearyl methoxycarbonylacetimidate hydrochloride

Выход 46.8%

Растворители

ethyl ether

Условия реакции

Обработка

1. 1
   ДругоеThe resulting white precipitates
2. 2
   Промывкаwere washed with ethylether
3. 3
   Другоеdried

Методика

In a mixture of 27.0 parts of stearyl alcohol in 200 volume parts of dry ethyl ether and 9.9 parts of methyl cyano acetate was introduced about 5.3 parts of dry hydrogen chloride gas at room temperature, followed by keeping at room temperature for 2 days. The resulting white precipitates were washed with ethylether and dried to give 19.0 parts of stearyl methoxycarbonylacetimidate hydrochloride melting at 83° to 85°C (decomposition). Yield: 46.8%

Источник