Реакция #351532
ord-2fd0cb85959e4ba889eb5e6891fecc2f
Уравнение реакции
methyl 2,5-dihydroxybenzoate
3,5,5-trimethylhexyl p-toluenesulfonate
→
methyl 5-(3,5,5-trimethylhexyloxy)-2-hydroxybenzoate
Выход 76.0%
Реагенты
Нет
Условия реакции
Подробные условия
See reaction.notes.procedure_details.
Обработка
- 1ДругоеSynthesis
Методика
Synthesis was carried out in the same manner as in Example 1, except for replacing methyl 2,4-dihydroxybenzoate with methyl 2,5-dihydroxybenzoate and replacing 2-ethylhexyl bromide with 3,5,5-trimethylhexyl p-toluenesulfonate, to obtain methyl 5-(3,5,5-trimethylhexyloxy)-2-hydroxybenzoate represented by the following chemical formula (hereinafter referred to as compound 10) as a colorless, clear and oily substance in a yield of 76%. The analytical results are shown below. ##STR31##