Реакция #349010

Уравнение реакции

2-methyl-3-chloroaniline

4-chlorobenzaldehyde

→

N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline

Условия реакции

Обработка

1. 1
   ТемператураThe mixture is heated
2. 2
   workup.DISTILLATIONDistillation at reduced pressure

Методика

2-methyl-3-chloroaniline (0.25 mole) and 4-chlorobenzaldehyde (0.25 mole) are ground in a mortar. The mixture is heated, with stirring in a water bath for 1.5 hours. Distillation at reduced pressure gives N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline; Bp. 139° C./0/020 mm.

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