Реакция #336822

ord-5ef4352b11c3443e87db73d3185b8e02

Уравнение реакции

CC(C)CCCC(C)CCO
3,7-dimethyl-1-octanol
CCOC(=O)C(C)O
ethyl lactate
CC(C)CCCC(C)CCOC(=O)C(C)O
3,7-dimethyl-1-octyl lactate
Выход 62.2%

Реагенты

Нет

Условия реакции

Температура
60°CELSIUS
Подробные условия
See reaction.notes.procedure_details.

Методика

A mixture of Novozym 435 (2.81 g), molecular sieves (23.17 g), 3,7-dimethyl-1-octanol (4.64 g), and ethyl lactate (14.78 g) in a 250 mL beaker was maintained at 60° C. in a convection oven for 28 hours. Upon work-up, 4.2 g of 3,7-dimethyl-1-octyl lactate (62% yield) was obtained as an amber-colored liquid. The purity of the product was >96% as assessed by HPLC-RI.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US07863025B2uspto-grants-2011_01