Реакция #335745

Уравнение реакции

formaldehyde dimethyl acetal

4-bromophenol

→

4-Methoxymethoxy-1-bromobenzene

Выход 49.0%

Условия реакции

Обработка

1. 1
   ДругоеFletcher, Synthesis 1976, p
2. 2
   Другоеthis derivative is 54° to 56° C. at 0.1 hPa

Методика

4-Methoxymethoxy-1-bromobenzene was prepared from formaldehyde dimethyl acetal and 4-bromophenol by the method of Y. P. Yardley and H. Fletcher, Synthesis 1976, p. 244. The boiling point of this derivative is 54° to 56° C. at 0.1 hPa, and the yield is 49 percent theory.

Источник