Реакция #334891

ord-d55c128e493543ae96f7edf2646d3d77

Уравнение реакции

O=C1OCCO1
ethylene carbonate
O=C1OCCO1
ethylene carbonate
Выход 97.5%
O=C=O
carbon dioxide
Выход 23.7%

Реактанты

Реагенты

Растворители

Условия реакции

Температура
175°CELSIUS
Подробные условия
See reaction.notes.procedure_details.

Методика

A 10:1 mole ratio of ethylene carbonate and diethylene glycol is heated with stirring under a nitrogen atmosphere for 3 hours at 175° C. using 0.5 percent Na2SnO3.3H2O as catalyst to give 97.5 percent ethylene carbonate conversion to a poly(alkylene carbonate) polyol with 23.7 percent carbon dioxide. The catalyst is removed as in Example 1.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US04709069uspto-grants-1987_11