Реакция #314574

ord-ed571ac63d0c4329805ce0dbf15561d7

Растворители

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Методика

The 4-(3-hydroxypropyl)morpholine (Aldrich, 0.18 g, 1.2 mmol), triethylamine (0.56 mL, 4.1 mmol), and methanesulfonyl chloride (0.15 mL, 1.9 mmol) in 10 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US07560481B2uspto-grants-2009_07