Реакция #3066

Уравнение реакции

ethyl 3-bromo-4-methylbenzoate

NBS

benzoyl peroxide

→

ethyl 3-bromo-4-bromomethylbenzoate

Растворители

CCl4

Условия реакции

Обработка

1. 1
   Температураwas refluxed for 4 h
2. 2
   Фильтрацияprocessed by filtration and chromatography

Методика

A mixture of 1.0 mmol of ethyl 3-bromo-4-methylbenzoate, 1.0 mmol NBS, and 0.02 mmol benzoyl peroxide in 5 mL CCl4 was refluxed for 4 h and then processed by filtration and chromatography to provide ethyl 3-bromo-4-bromomethylbenzoate as an oil.

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