Реакция #2676

Уравнение реакции

alcohol

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styrol

m-chloro perbenzoic acid

→

expected product

Выход 99.6%

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-(1,2-epoxy) styrol

Выход 99.6%

Растворители

AcOEt cyclohexane

cyclo-hexane ethyl acetate

Условия реакции

Обработка

1. 1
   Другоеwere reacted

Методика

Using the procedure of Stage D of Example 40, 13.2 g of thee allylic alcohol of Step C and 10.3 g of m-chloro perbenzoic acid were reacted to obtain 13.7 g of the expected product with a Rf=0.25 (AcOEt-cyclohexane 6-4).

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