Реакция #2467931
ord-805213d305c74b3da5b5bcfb7dfd9ad1
Уравнение реакции
sodium hydroxide
melamine
dimethoxyethanal
→
Melamine Dimethoxyethanal
Реагенты
Нет
Условия реакции
Температура
52.5°CELSIUS
Подробные условия
See reaction.notes.procedure_details.
Обработка
- 1ТемператураThis mixture was heated
- 2Температураwhile maintaining the pH
- 3Другоеclose to 9-9.5 with adjustment
Методика
200 g of melamine (1.59 mol) were added to 580 g of a 60% aqueous solution of dimethoxyethanal (3.35 mol). This mixture was heated under stirring for 2 h at 50-55° C. while maintaining the pH close to 9-9.5 with adjustment, if necessary, with as much 20% sodium hydroxide as was required (about 7 g).