Реакция #2389088

Уравнение реакции

dodecane thiol

chloride

→

dodecansulfenyl chloride

Растворители

CHCl3

Условия реакции

Обработка

1. 1
   ДругоеRemoval of solvent (aspirator)

Методика

To a solution of dodecane thiol (1.00 mL, 4.17 mmol, Aldrich) in 20 mL CHCl3 was added suliryl chloride (0.74 mL, 9.19 mmol, Aldrich), and the regulting mixture was stirred at room temperature for 18 h. Removal of solvent (aspirator), afforded dodecansulfenyl chloride that was determined to be sufficiently pure by 1H NMR.

Источник