Реакция #2383779

Уравнение реакции

Pentafluorobenzenesulfonyl chloride

tetramethylammonium hydroxide

→

pentafluorobenzenesulfonic acid tetramethylammonium salt

Растворители

methanol

Условия реакции

Обработка

1. 1
   Температураcooling

Методика

Pentafluorobenzenesulfonyl chloride (25 g) was dissolved in 100 ml of methanol with ice-cooling, and 100 g of a 25% aqueous solution of tetramethylammonium hydroxide was gradually added thereto. The reaction mixture was stirred at room temperature for 3 hours, thereby a solution of a pentafluorobenzenesulfonic acid tetramethylammonium salt was obtained. This solution was used for salt exchange of a sulfonium salt and an iodonium salt.

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