Реакция #2383768

Уравнение реакции

N,N-bis-(tert-butoxycarboxy-methyl)-S-ethyl-2-mercaptoethylamine

hydrochloric acid

→

N,N-Bis-(hydroxycarboxy-methyl)-S-ethyl-2-mercaptoethylamine-hydrochloride

Растворители

tetrahydrofuran

Условия реакции

Обработка

1. 1
   ДругоеThe resulting reaction mixture
2. 2
   Концентрированиеconcentrated by evaporation in a vacuum
3. 3
   ФильтрацияThen, the product is filtered off
4. 4
   Другоеdried in a medium-high vacuum

Методика

1.67 g (5 mmol) of N,N-bis-(tert-butoxycarboxy-methyl)-S-ethyl-2-mercaptoethylamine is dissolved in 12 ml of tetrahydrofuran and mixed with 6 ml of concentrated hydrochloric acid. The resulting reaction mixture is stirred for 1 hour at room temperature and concentrated by evaporation in a vacuum. The residue is pulverized with 10 ml of absolute diethyl ether. Then, the product is filtered off and dried in a medium-high vacuum.

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