Реакция #2358504

Уравнение реакции

propylene glycol

propylene glycol

tetrahydrofuran

→

propylene glycol THF

Условия реакции

Обработка

1. 1
   workup.ADDITIONmixture of silica gel

Методика

Activated silica gel of step (1) and tetrahydrofuran are stirred at ambient temperature, then 70 ml of propylene glycol is added (adding 0.2 ml of propylene glycol per gram of silica gel) at ambient temperature, after stirring 1 hour the temperature is raised to 40° C., then mixture of silica gel HHV-4/propylene glycol/THF is obtained;

Источник