Реакция #2320116

ord-977ef84577d2439fbb7cbd128d3f00bf

Уравнение реакции

Clc1ccc(Br)cc1Cl
4-bromo-1,2-dichlorobenzene
C1CNCCN1
piperazine
Clc1ccc(N2CCNCC2)cc1Cl
title compound
Выход 48.2%
Clc1ccc(N2CCNCC2)cc1Cl
1-(3,4-dichloro-phenyl)-piperazine
Выход 48.2%

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Методика

Beginning with 4-bromo-1,2-dichlorobenzene (200 mg, 0.88 mmol) and piperazine (91 mg, 1.06 mmol), 98 mg of the title compound was recovered by the procedure described in Example 1.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: USRE041315E1uspto-grants-2010_05