Реакция #2195502

Уравнение реакции

product

9-Benzyl-7,7,11,11-tetrafluoro-1,5-dithia-9-azaspiro[5.5]undecane

→

title compound

1-Benzyl-3,3,5,5-tetrafluoropiperidine

Условия реакции

Обработка

1. 1
   Другоеpurify by silica gel chromatography

Методика

React 4.0 mmol of the product of Example 29 with Raney nickel according to the general procedure set forth in Example 23 and purify by silica gel chromatography using methylene chloride/methanol/saturated NH4OH as eluant to yield the title compound.

Источник