Реакция #2195500

Уравнение реакции

product

Diethyl 2,2′-(1,3-dithiane-2,2-diyl)bis(2,2-difluoroacetate)

benzylamine

→

title compound

9-Benzyl-7,7,11,11-tetrafluoro-1,5-dithia-9-azaspiro[5.5]undecane-8,10-dione

Условия реакции

Обработка

1. 1
   Другоеpurify by silica gel chromatography

Методика

React 7.2 mmol of the product of Example 20 with benzylamine using the general procedure set forth in Example 8, and purify by silica gel chromatography using ethyl acetate/hexane as eluant to yield the title compound.

Источник