Реакция #2171029

Уравнение реакции

1,3-bis-(3,5-dibromo-4-nitropyrazol-1-yl)propane

1,3-bis-(3,5-dibromo-4-nitro-pyrazol-1-yl)propane

benzylamine

water

→

1,3-bis-(5-benzylamino-3-bromo-4-nitropyrazol-1-yl)-propane

Растворители

n-propanol

Условия реакции

Обработка

1. 1
   ТемператураSubsequently the reaction mixture is cooled
2. 2
   ФильтрацияThe precipitate is filtered with suction
3. 3
   Промывкаwashed with water
4. 4
   Другоеdried in vacuum at 60° C.

Методика

11.6 g of 1,3-bis-(3,5-dibromo-4-nitropyrazol-1-yl)propane from step 5.1 are heated together with 6.5 g of benzylamine in 180 ml of n-propanol for 1 hour at 100° C. Subsequently the reaction mixture is cooled and poured into 1000 ml water. The precipitate is filtered with suction, washed with water and dried in vacuum at 60° C.

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