Реакция #216833

Уравнение реакции

diphenyliodonium chloride

lithium tetrakis(pentafluorophenyl)borate

→

diphenyliodonium tetrakis(pentafluorophenyl)borate

Выход 75.0%

Растворители

water

water

Условия реакции

Обработка

1. 1
   ТемператураThe mixture was maintained
2. 2
   Фильтрацияwas then filtered
3. 3
   ДругоеThe filtrate was dried under reduced pressure (133 Pa) overnight with the exclusion of light
4. 4
   Другое16.33 g (or a yield of 75%) of diphenyliodonium tetrakis(pentafluorophenyl)borate were thus recovered

Методика

7.17 g (or 22.6 mmol) of diphenyliodonium chloride were dissolved in 300 ml of water in a 1,000 ml Erlenmeyer flask. 15.52 g (or 22.6 mmol) of lithium tetrakis(pentafluorophenyl)borate in solution in 250 ml of water were added dropwise. The mixture was maintained under stirring for 30 minutes and was then filtered. The filtrate was dried under reduced pressure (133 Pa) overnight with the exclusion of light. 16.33 g (or a yield of 75%) of diphenyliodonium tetrakis(pentafluorophenyl)borate were thus recovered.

Источник