Реакция #2074997

Уравнение реакции

6-Bromo-naphthalene-2-carbonyl chloride

N-(4-amino-benzothiazol-2-yl)-acetamide

→

title compound

6-Bromo-naphthalene-2-carboxylic acid (2-acetylamino-benzothiazol-4-yl)-amide

Условия реакции

Обработка

1. 1
   ДругоеThis material was prepared analogous to the procedure
2. 2
   Другоеprepared

Методика

This material was prepared analogous to the procedure described for Example 1(b). 6-Bromo-naphthalene-2-carbonyl chloride, Example 1(a), (98 mg, 0.36 mmol) reacted with N-(4-amino-benzothiazol-2-yl)-acetamide (50 mg, 0.24 mmol, prepared according to the procedure described in WO03099284) to give the title compound as a solid. Mp 241.6° C. MS (ESI, pos. ion.) m/z: 441 (M+1).

Источник