Реакция #1973965

Уравнение реакции

4-chloro-3-nitroaniline

methanesulfonyl chloride

pyridine

→

title compound

Выход 92.2%

N-(4-chloro-3-nitrophenyl)methanesulfonamide

Выход 92.2%

Растворители

THF

HCl

Условия реакции

Обработка

1. 1
   ФильтрацияThe resulting precipitate was filtered
2. 2
   Другоеair-dried

Методика

A mixture of 4-chloro-3-nitroaniline (5.0 g, 29 mmol), methanesulfonyl chloride (2.37 mL, 30.4 mmol) and pyridine (5.9 mL, 72.4 mmol) in THF (100 mL) was stirred for 24 h. Poured in 1M HCl (500 mL). The resulting precipitate was filtered and air-dried to provide the title compound as a solid (6.7 g, 92%).

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