Реакция #1973963

Уравнение реакции

3,4-dinitroaniline

methanesulfonyl chloride

pyridine

→

title compound

N-(3,4-dinitrophenyl)methanesulfonamide

Растворители

CH2Cl2

Условия реакции

Обработка

1. 1
   КонцентрированиеMixture was concentrated under vacuum

Методика

A mixture of 3,4-dinitroaniline (5.27 g, 28.8 mmol), methanesulfonyl chloride (3.36 mL, 43.1 mmol) and pyridine (5.82 mL, 71.9 mmol) in CH2Cl2 (100 mL) was stirred for 24 h. Mixture was concentrated under vacuum to provide a crude semi-solid title compound that was used without further purification.

Источник