Реакция #1904039

Уравнение реакции

hydroxy amine

glutaric anhydride

→

Hydroxylamine Glutarate

Растворители

benzene

triethyl amine

Условия реакции

Обработка

1. 1
   Температураrefluxed for 2 h
2. 2
   ДругоеThe solvent is evaporated under vacuum
3. 3
   Другоеthe residue is purified by flash chromatography

Методика

This example that demonstrates how this method could be performed. Part 1: To a solution of 2 g hydroxy amine in 100 ml dry benzene and 20 ml triethyl amine, 9.4 g glutaric anhydride is added and the reaction mixture stirred at room temperature for 2 h and refluxed for 2 h. The solvent is evaporated under vacuum and the residue is purified by flash chromatography using silica gel.

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