Реакция #1883849

Уравнение реакции

compound 426B

3-Chloro-4-(1-methyl-1H-imidazol-2-ylsulfanyl)-phenylamine

3-fluoro-4-nitro-phenol

→

Compound 427A

Выход 92.3%

4-Amino-3-fluoro-phenol

Выход 92.3%

Условия реакции

Обработка

1. 1
   Другоеa retention time of 4.79 min (standard LC1 method, 8 min run)

Методика

Compound 427A (1.49 g, 92%) was prepared from 3-fluoro-4-nitro-phenol (2.0 g, 12.7 mmol) by a route analogous to that used for the preparation of compound 426B. It is a yellow solid and has a retention time of 4.79 min (standard LC1 method, 8 min run). MS Found: (M+H)+=128.1

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