Реакция #1876821

ord-a9e2bc7ece64422aa680ac0d6978bd7c

Растворители

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    ДругоеReaction
  2. 2
    Другоеwas carried out at room temperature

Методика

The 1,3-dichloroformyl-5-hydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an eguimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature to obtain 1,3-dichloroformyl-5-trimethylsiloxyadamantane.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US07070905B2uspto-grants-2006_07