Реакция #1860

ord-d735999e237040e79efd9e34aa9e36bf

Уравнение реакции

CCOC(=O)CBr
ethyl bromoacetate
CSC
dimethyl sulfide
CCOC(=O)C[S+](C)C.[Br-]
title compound
CCOC(=O)C[S+](C)C.[Br-]
Carboethoxymethyl Dimethylsulfonium Bromide

Реагенты

Нет

Растворители

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Методика

A solution of ethyl bromoacetate (265 g) and dimethyl sulfide (114 g) in acetone (500 mL) was stirred at room temperature. After three days, the title compound was isolated by filtration of the reaction mixture. Melting point 88°-90° C.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US05726320uspto-grants-1998_03