Реакция #1771990

ord-56238b79bf8e4876a8c816dff94dc2f6

Уравнение реакции

CC1(C)CN(C(=O)OC(C)(C)C)[C@@](C(=O)O)(C(C)(C)C)C1
tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline
CC1(C)CN[C@H](C(=O)O)C1
4,4-Dimethylproline

Реагенты

Нет

Растворители

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    КонцентрированиеThe solution was concentrated
  2. 2
    Другоеdried under high vacuum
  3. 3
    Другоеtaken to the next step without further purification

Методика

A solution of tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline in dichloromethane (5 mL) and trifluoroacetic (5 mL) was stirred at room temperature for five hours. The solution was concentrated, dried under high vacuum and taken to the next step without further purification.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: USRE043298E1uspto-grants-2012_04