Реакция #1710838

Уравнение реакции

methyl 2,5-dihydroxybenzoate

potassium carbonate

TsCl

→

Methyl 2-hydroxy-5-{[(4-methylphenyl)sulfonyl]oxy}benzoate

Растворители

acetone

Условия реакции

Обработка

1. 1
   Температураthe mixture was refluxed for 7 h

Методика

A mixture of methyl 2,5-dihydroxybenzoate (1.5 g, 8.92 mmol), potassium carbonate (7.50 g, 54.2 mmol), and dry acetone (100 ml) was stirred at room temperature for 30 min. To the mixture was added TsCl (1.72 g, 9.00 mmol) portionwise and the mixture was refluxed for 7 h. The reaction mixture was used in the next step directly.

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