Реакция #1687635

Уравнение реакции

fumarate

88

5-Methyl-2-(3-pyridyl)-thiazole

→

title compound

5-Methyl-2-(1-methyl-1,2,5,6-tetrahydro-3-pyridyl)-thiazole

Условия реакции

Обработка

1. 1
   ДругоеThe crude free base obtained

Методика

The title compound was prepared from 88 (2.2 g, 0.013 mol) by the procedure described in Example 49. The crude free base obtained, 89, was converted to the title fumarate, 90. Yield: 0.8 g (0.0032 mol, 25%). M.P. 159°-160° C. Anal. (C12H16N2O2S)C, H, N.

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