Реакция #166962

Уравнение реакции

6-Bromonaphthalene-2-carboxylic acid

thionyl chloride

→

6-bromonaphthalene-2-carbonyl chloride

Условия реакции

Обработка

1. 1
   Другоеevaporated under vacuum
2. 2
   workup.DISSOLUTIONSolid was dissolved in dichloromethane (50 mL)
3. 3
   Другоеevaporated under vacuum

Методика

6-Bromonaphthalene-2-carboxylic acid (25.1 g) was suspended in thionyl chloride (200 mL), stirred at 60° C. for 16 hours and evaporated under vacuum. Solid was dissolved in dichloromethane (50 mL) and evaporated under vacuum, giving 6-bromonaphthalene-2-carbonyl chloride (27.0 g, crude) as a white solid.

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