Реакция #1609

Уравнение реакции

p-chlorobenzoic hydrazide

chloroacetyl chloride

→

N'-chloroacetyl-4-chlorobenzoic hydrazide

Растворители

dioxane

Условия реакции

Обработка

1. 1
   ТемператураThe resulting mixture was refluxed for three hours
2. 2
   Фильтрацияfiltered
3. 3
   ПромывкаThe resulting solid was washed with ethyl ether
4. 4
   Другоеdried

Методика

To a solution of p-chlorobenzoic hydrazide (11.2 g) in dioxane (100 ml) was added chloroacetyl chloride (6 ml). The resulting mixture was refluxed for three hours cooled to room temperature and filtered. The resulting solid was washed with ethyl ether and dried to yield N'-chloroacetyl-4-chlorobenzoic hydrazide as white solid.

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