Реакция #160780

ord-e89532cfc9aa4bf1a9d4183dc46c277c

Уравнение реакции

NC(=O)C1CCCCC1
cyclohexanecarboxamide
COc1ccc(P2(=S)SP(=S)(c3ccc(OC)cc3)S2)cc1
Lawesson's reagent
→
NC(=S)C1CCCCC1
cyclohexanecarbothioamide

Реактанты

NC(=O)C1CCCCC1
cyclohexanecarboxamide
COc1ccc(P2(=S)SP(=S)(c3ccc(OC)cc3)S2)cc1
Lawesson's reagent

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    Другоеwere reacted

Методика

Following Method 3, cyclohexanecarboxamide and Lawesson's reagent were reacted, yielding cyclohexanecarbothioamide. LCMS (m/z): 144.1 (MH+); LC Rt=5.10 min.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US08829193B2uspto-grants-2014_09