Реакция #155395

Уравнение реакции

3-tert-butyldimethylsilyloxybenzoic acid

thionyl chloride

→

3-tert-Butyldimethylsilyloxybenzoyl chloride

Условия реакции

Обработка

1. 1
   Температураwas heated
2. 2
   Температураat reflux for 90 mins
3. 3
   КонцентрированиеThe reaction mixture was concentrated under reduced pressure
4. 4
   Другоеto give an oil
5. 5
   Другоеyield 5.77 parts of the following structure

Методика

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 90 mins. The reaction mixture was concentrated under reduced pressure to give an oil, yield 5.77 parts of the following structure.

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