Реакция #1552054

Уравнение реакции

methyl-4-bromobenzoate

hydrazine monohydrate

→

white solid

Выход 67.0%

4-bromobenzohydrazide

Выход 67.0%

Растворители

ethanol

Условия реакции

Обработка

1. 1
   Температураthe mixture was heated
2. 2
   workup.STIRRINGstirred at 78° C. for 5 hours
3. 3
   ДругоеA solid obtained
4. 4
   Промывкаwashed with water
5. 5
   Фильтрацияcollected by suction filtration

Методика

First, 3.0 g (13.9 mmol) of methyl-4-bromobenzoate was put in a 100-mL three-neck flask, 10 mL of ethanol was added therein, and the mixture was stirred. Thereafter, 4.0 mL of hydrazine monohydrate was added therein, and the mixture was heated and stirred at 78° C. for 5 hours. A solid obtained washed with water and collected by suction filtration; thus, 2.0 g of a white solid of objective 4-bromobenzohydrazide was obtained (yield: 67%).

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