Реакция #1552050

Уравнение реакции

1,8-octanediamine

triethylamine

furoyl chloride

→

N,N′-(octane-1,8-diyl)bis(furan-2-carboxamide)

Условия реакции

Обработка

1. 1
   ДругоеThe resulting compound was purified by column chromatography (98:2 DCM:EtOAc)
2. 2
   Другоеthe product obtained as a white solid (21.5 g/92%)

Методика

The general procedure was carried out using 1,8-octanediamine (10.0 g, 69.3 mmol), triethylamine (14.2 g, 141 mmol), DMAP (0.17 g, 1.35 mmol) and furoyl chloride (19.0 g, 146 mmol). The resulting compound was purified by column chromatography (98:2 DCM:EtOAc), and the product obtained as a white solid (21.5 g/92%).

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