Реакция #1552043

Уравнение реакции

N-methoxy-acrylamide

chloroformic acid vinyl ester

→

title compound

N-Methoxy-N-propenoylcarbamic acid vinyl ester

Условия реакции

Обработка

1. 1
   ДругоеPurification by column chromatography on silica gel (PE:EE=9:1)

Методика

The synthesis was carried out analogously to synthesis example 8 using N-methoxy-acrylamide and chloroformic acid vinyl ester. Purification by column chromatography on silica gel (PE:EE=9:1) yielded 1.6 g (91% of th.) of the title compound as a colorless liquid.

Источник