Реакция #1537541

Уравнение реакции

product

1,4-Dioxa-8-thiaspiro[4.5]decan-7-ol

thioacetic acid

p-toluene-sulfonic acid

→

desired product

Ethanethioic Acid S-(1,4-Dioxa-8-thiaspiro[4.5]decan-7-yl) Ester

Растворители

carbon tetrachloride

Условия реакции

Обработка

1. 1
   КонцентрированиеAfter work up concentration in vacuo

Методика

A mixture of 0.545 g of product from Example 394, 0.23 ml of thioacetic acid, 0.16 g of p-toluene-sulfonic acid and 8 ml of carbon tetrachloride is stirred at room temperature for 1 hour. After work up concentration in vacuo gives 0.556 g of the desired product.

Источник