Реакция #1256745

Уравнение реакции

Compound 40a

Isobutyldiisopropylsilane

diisopropylchlorosilane

→

Compound 44a

Cyclopropyldiisopropylsilane

Растворители

Условия реакции

Методика

The procedure of synthesizing Compound 40a was repeated, except that diisopropylchlorosilane (4.10 mL, 96.0 mmol) and cyclopropylmagnesium bromide THF solution (1.0M, 100 mL) were employed, whereby the Compound 44a was obtained as a colorless liquid (boiling point; 35 mmHg, 86 to 89° C. fraction, 1.84 g, 50%).

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