Реакция #1135813

ord-0124a7c0ff9a437f91fc0767421e3bb0

Уравнение реакции

CCOc1cccc([N+](=O)[O-])c1C
1-ethoxy-2-methyl-3-nitrobenzene
CCOc1cccc(N)c1C
3-ethoxy-2-methylaniline

Реагенты

Растворители

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    ФильтрацияThe mixtures were filtered
  2. 2
    Концентрированиеthe filtrates were concentrated

Методика

A mixture of 1-ethoxy-2-methyl-3-nitrobenzene described in Reference Preparation example 2539.9 g, palladium-carbon (palladium 5%) 4 g and ethanol 200 mL was stirred at room temperature under hydrogen atmosphere for eighteen hours. The mixtures were filtered and the filtrates were concentrated to give 3-ethoxy-2-methylaniline 33.0 g.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US09380782B2uspto-grants-2016_07