Реакция #1135813
ord-0124a7c0ff9a437f91fc0767421e3bb0
Уравнение реакции
1-ethoxy-2-methyl-3-nitrobenzene
→
3-ethoxy-2-methylaniline
Реактанты
Реагенты
Растворители
Условия реакции
Подробные условия
See reaction.notes.procedure_details.
Обработка
- 1ФильтрацияThe mixtures were filtered
- 2Концентрированиеthe filtrates were concentrated
Методика
A mixture of 1-ethoxy-2-methyl-3-nitrobenzene described in Reference Preparation example 2539.9 g, palladium-carbon (palladium 5%) 4 g and ethanol 200 mL was stirred at room temperature under hydrogen atmosphere for eighteen hours. The mixtures were filtered and the filtrates were concentrated to give 3-ethoxy-2-methylaniline 33.0 g.